Multivariate optimization of a spectrophotometric method for copper determination in Brazilian sugar-cane spirits using the Doehlert design
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A Rapid and Sensitive Method for Dimethylsulphide Analysis in Brazilian Sugar Cane Sugar Spirits and Other Distilled Beverages
O acoplamento do extrator por “purge and trap” com a cromatografia gasosa foi utilizado para quantificar o dimetilssulfeto em bebidas alcoólicas. Muito boa performance foi obtida usando-se uma coluna HP-FFAP e um detector seletivo de massas operando em modo SIM (m/z 62): limite de detecção de 8 x 10 mol L; boa repetibilidade e tempo total de análise de 25 minutos. O método foi aplicado em 60 am...
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ژورنال
عنوان ژورنال: Microchemical Journal
سال: 2011
ISSN: 0026-265X
DOI: 10.1016/j.microc.2011.04.008